Validated Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry Method for Analyzing LSD, iso-LSD, nor-LSD, and O-H-LSD in Blood and Urine
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چکیده
منابع مشابه
Effective GC-MS procedure for detecting iso-LSD in urine after base-catalyzed conversion to LSD.
A sensitive method is described to detect isolysergic acid diethylamide (iso-LSD) in urine. The compound was extracted from urine and converted to a C-8 carbanion by sodium ethoxide in ethanol. Protonation of the carbanion by water selectively produced LSD. The conversion of iso-LSD to LSD was almost quantitative (98%). The product was purified by solid-phase fractionation and acid-base separat...
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ژورنال
عنوان ژورنال: Journal of Analytical Toxicology
سال: 2009
ISSN: 0146-4760,1945-2403
DOI: 10.1093/jat/33.5.253